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Beilstein J. Org. Chem. 2019, 15, 218–235, doi:10.3762/bjoc.15.21
Graphical Abstract
Scheme 1: Multiblock copolymer synthesis by sequential ROMP, replotted from [51].
Figure 1: The most known commercially available catalysts for olefin metathesis.
Scheme 2: Multiblock copolymer synthesis by combining ROMP and NMP, replotted from [56].
Figure 2: A highly fluorescent multiblock copolymer for bioimaging and in vivo tumor targeting [60].
Scheme 3: Multiblock copolymer synthesis by combining ROMP and click reactions replotted from [61].
Scheme 4: Multiblock copolymer synthesis by combining ADMET and other reactions, replotted from [63,64].
Scheme 5: Synthesis of multiblock bottle-brush copolymers by ROMP, replotted from [68].
Scheme 6: Sacrificial synthesis of multiblock copolymers, replotted from [70].
Scheme 7: Synthesis of supramolecular multiblock copolymers, replotted from [74].
Figure 3: The multiblock copolymer capable of post-functionalization [76].
Figure 4: Multiblock copolymers synthesized by macromolecular cross metathesis.
Scheme 8: Macromolecular cross metathesis.
Figure 5: Changes in the DSC thermograms during MCM of PBD and polyesters (left) [84] and PNB–PCOE (right) mediat...
Figure 6: The 13C NMR spectrum recorded after 8 h of the reaction between PCOE, PNB, and Gr1; the homo- and h...
Scheme 9: Elementary reactions of MCM between PNB and PCOE, replotted from [90].
Figure 7: The 1H NMR spectrum recorded after 24 h of the reaction between PCOE, PNB, and Gr1 in CDCl3. The ca...
Scheme 10: Post-modification of multiblock copolymers by hydrogenation (A) [85] and epoxidation (B) [101] of C=C double...
Figure 8: Integral distribution functions for the lamella thickness of crystallites in thermally fractionated...
Beilstein J. Org. Chem. 2015, 11, 1796–1808, doi:10.3762/bjoc.11.195
Figure 1: Dependences of the (blue) PCOE and (green) PNB mean hydrodynamic radius in CHCl3 on the (a) light ...
Figure 2: Hydrodynamic radius distributions (normalized by their maximum values) in the CHCl3 solutions of (b...
Figure 3: Stability of the primary carbene [Ru]=CHPh in the pure solvent (CDCl3).
Scheme 1: Formation of polyoctenamer-bound carbene by the interaction of Gr-1 with PCOE.
Figure 4: (a) Dependences of the normalized (red) [Ru]=CHPh and (blue) [Ru]=PCOE carbene concentrations on ti...
Scheme 2: Formation of polynorbornene-bound carbene by the interaction of Gr-1 with PNB.
Figure 5: (a) Dependences of the normalized (red) [Ru]=CHPh and (green) [Ru]=PNB carbene concentrations on ti...
Scheme 3: Elementary cross-metathesis reactions in the mixture of PCOE with PNB.
Figure 6: Dependences of the normalized (red) primary, (blue) PCOE, and (green) PNB carbene concentrations an...
Figure 7: The kinetics of NB-COE dyads formation under mixing conditions for the systems with (red) cin/cp = ...
Figure 8: The 1H NMR spectrum recorded after 10 min of the reaction between PCOE and Gr-1 at the initial conc...
Figure 9: The 1H NMR spectrum recorded after 653 min of the reaction between PNB and Gr-1 at the initial conc...
Figure 10: The 1H NMR spectrum recorded after 24 h of the reaction between PCOE, PNB, and Gr-1 at the initial ...
Figure 11: The 13C NMR spectrum recorded after 8 h of the reaction between PCOE, PNB, and Gr-1 at the initial ...